Interlaboratory study of the operational stability of automated sorption balances

Research output: Contribution to journal › Journal article › Research › peer-review

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Interlaboratory study of the operational stability of automated sorption balances. / Zelinka, Samuel L.; Glass, Samuel V.; Lazarcik, Eleanor Q.D.; Thybring, Emil E.; Altgen, Michael; Rautkari, Lauri; Curling, Simon; Cao, Jinzhen; Wang, Yujiao; Künniger, Tina; Nyström, Gustav; Dreimol, Christopher Hubert; Burgert, Ingo; Uyup, Mohd Khairun Anwar; Khadiran, Tumirah; Roper, Mark G.; Broom, Darren P.; Schwarzkopf, Matthew; Yudhanto, Arief; Subah, Mohammad; Lubineau, Gilles; Fredriksson, Maria; Strojecki, Marcin; Olek, Wiesław; Majka, Jerzy; Pedersen, Nanna Bjerregaard; Burnett, Daniel J.; Garcia, Armando R.; Verdonck, Els; Dreisbach, Frieder; Waguespack, Louis; Schott, Jennifer; Esteban, Luis G.; Garcia-Iruela, Alberto; Colinart, Thibaut; Rémond, Romain; Mazian, Brahim; Perre, Patrick; Emmerich, Lukas; Li, Ling.

In: Adsorption, 2024.

Research output: Contribution to journal › Journal article › Research › peer-review

Harvard

Zelinka, SL, Glass, SV, Lazarcik, EQD, Thybring, EE, Altgen, M, Rautkari, L, Curling, S, Cao, J, Wang, Y, Künniger, T, Nyström, G, Dreimol, CH, Burgert, I, Uyup, MKA, Khadiran, T, Roper, MG, Broom, DP, Schwarzkopf, M, Yudhanto, A, Subah, M, Lubineau, G, Fredriksson, M, Strojecki, M, Olek, W, Majka, J, Pedersen, NB, Burnett, DJ, Garcia, AR, Verdonck, E, Dreisbach, F, Waguespack, L, Schott, J, Esteban, LG, Garcia-Iruela, A, Colinart, T, Rémond, R, Mazian, B, Perre, P, Emmerich, L & Li, L 2024, 'Interlaboratory study of the operational stability of automated sorption balances', Adsorption. https://doi.org/10.1007/s10450-024-00472-9

APA

Zelinka, S. L., Glass, S. V., Lazarcik, E. Q. D., Thybring, E. E., Altgen, M., Rautkari, L., Curling, S., Cao, J., Wang, Y., Künniger, T., Nyström, G., Dreimol, C. H., Burgert, I., Uyup, M. K. A., Khadiran, T., Roper, M. G., Broom, D. P., Schwarzkopf, M., Yudhanto, A., ... Li, L. (2024). Interlaboratory study of the operational stability of automated sorption balances. Adsorption. https://doi.org/10.1007/s10450-024-00472-9

Vancouver

Zelinka SL, Glass SV, Lazarcik EQD, Thybring EE, Altgen M, Rautkari L et al. Interlaboratory study of the operational stability of automated sorption balances. Adsorption. 2024. https://doi.org/10.1007/s10450-024-00472-9

Author

Zelinka, Samuel L. ; Glass, Samuel V. ; Lazarcik, Eleanor Q.D. ; Thybring, Emil E. ; Altgen, Michael ; Rautkari, Lauri ; Curling, Simon ; Cao, Jinzhen ; Wang, Yujiao ; Künniger, Tina ; Nyström, Gustav ; Dreimol, Christopher Hubert ; Burgert, Ingo ; Uyup, Mohd Khairun Anwar ; Khadiran, Tumirah ; Roper, Mark G. ; Broom, Darren P. ; Schwarzkopf, Matthew ; Yudhanto, Arief ; Subah, Mohammad ; Lubineau, Gilles ; Fredriksson, Maria ; Strojecki, Marcin ; Olek, Wiesław ; Majka, Jerzy ; Pedersen, Nanna Bjerregaard ; Burnett, Daniel J. ; Garcia, Armando R. ; Verdonck, Els ; Dreisbach, Frieder ; Waguespack, Louis ; Schott, Jennifer ; Esteban, Luis G. ; Garcia-Iruela, Alberto ; Colinart, Thibaut ; Rémond, Romain ; Mazian, Brahim ; Perre, Patrick ; Emmerich, Lukas ; Li, Ling. / Interlaboratory study of the operational stability of automated sorption balances. In: Adsorption. 2024.

Bibtex

@article{2ba3fd229e3f450cbb6f85be5899b2db,
title = "Interlaboratory study of the operational stability of automated sorption balances",
abstract = "Automated sorption balances are widely used for characterizing the interaction of water vapor with hygroscopic materials. These instruments provide an efficient way to collect sorption isotherm data and kinetic data. A typical method for defining equilibrium after a step change in relative humidity (RH) is using a particular threshold value for the rate of change in mass with time. Recent studies indicate that commonly used threshold values yield substantial errors and that further measurements are needed at extended hold times as a basis to assess the accuracy of abbreviated equilibration criteria. However, the mass measurement accuracy at extended times depends on the operational stability of the instrument. Published data on the stability of automated sorption balances are rare. An interlaboratory study was undertaken to investigate equilibration criteria for automated sorption balances. This paper focuses on the mass, temperature, and RH stability and includes data from 25 laboratories throughout the world. An initial target for instrument mass stability was met on the first attempt in many cases, but several instruments were found to have unexpectedly large instabilities. The sources of these instabilities were investigated and greatly reduced. This paper highlights the importance of verifying operational mass stability of automated sorption balances, gives a method to perform stability checks, and provides guidance on identifying and correcting common sources of mass instability.",
keywords = "Interlaboratory investigation, Measurement uncertainty, Water vapor sorption",
author = "Zelinka, {Samuel L.} and Glass, {Samuel V.} and Lazarcik, {Eleanor Q.D.} and Thybring, {Emil E.} and Michael Altgen and Lauri Rautkari and Simon Curling and Jinzhen Cao and Yujiao Wang and Tina K{\"u}nniger and Gustav Nystr{\"o}m and Dreimol, {Christopher Hubert} and Ingo Burgert and Uyup, {Mohd Khairun Anwar} and Tumirah Khadiran and Roper, {Mark G.} and Broom, {Darren P.} and Matthew Schwarzkopf and Arief Yudhanto and Mohammad Subah and Gilles Lubineau and Maria Fredriksson and Marcin Strojecki and Wies{\l}aw Olek and Jerzy Majka and Pedersen, {Nanna Bjerregaard} and Burnett, {Daniel J.} and Garcia, {Armando R.} and Els Verdonck and Frieder Dreisbach and Louis Waguespack and Jennifer Schott and Esteban, {Luis G.} and Alberto Garcia-Iruela and Thibaut Colinart and Romain R{\'e}mond and Brahim Mazian and Patrick Perre and Lukas Emmerich and Ling Li",
note = "Publisher Copyright: {\textcopyright} This is a U.S. Government work and not under copyright protection in the US; foreign copyright protection may apply 2024.",
year = "2024",
doi = "10.1007/s10450-024-00472-9",
language = "English",
journal = "Adsorption",
issn = "0929-5607",
publisher = "Springer",

}

RIS

TY - JOUR

T1 - Interlaboratory study of the operational stability of automated sorption balances

AU - Zelinka, Samuel L.

AU - Glass, Samuel V.

AU - Lazarcik, Eleanor Q.D.

AU - Thybring, Emil E.

AU - Altgen, Michael

AU - Rautkari, Lauri

AU - Curling, Simon

AU - Cao, Jinzhen

AU - Wang, Yujiao

AU - Künniger, Tina

AU - Nyström, Gustav

AU - Dreimol, Christopher Hubert

AU - Burgert, Ingo

AU - Uyup, Mohd Khairun Anwar

AU - Khadiran, Tumirah

AU - Roper, Mark G.

AU - Broom, Darren P.

AU - Schwarzkopf, Matthew

AU - Yudhanto, Arief

AU - Subah, Mohammad

AU - Lubineau, Gilles

AU - Fredriksson, Maria

AU - Strojecki, Marcin

AU - Olek, Wiesław

AU - Majka, Jerzy

AU - Pedersen, Nanna Bjerregaard

AU - Burnett, Daniel J.

AU - Garcia, Armando R.

AU - Verdonck, Els

AU - Dreisbach, Frieder

AU - Waguespack, Louis

AU - Schott, Jennifer

AU - Esteban, Luis G.

AU - Garcia-Iruela, Alberto

AU - Colinart, Thibaut

AU - Rémond, Romain

AU - Mazian, Brahim

AU - Perre, Patrick

AU - Emmerich, Lukas

AU - Li, Ling

N1 - Publisher Copyright: © This is a U.S. Government work and not under copyright protection in the US; foreign copyright protection may apply 2024.

PY - 2024

Y1 - 2024

N2 - Automated sorption balances are widely used for characterizing the interaction of water vapor with hygroscopic materials. These instruments provide an efficient way to collect sorption isotherm data and kinetic data. A typical method for defining equilibrium after a step change in relative humidity (RH) is using a particular threshold value for the rate of change in mass with time. Recent studies indicate that commonly used threshold values yield substantial errors and that further measurements are needed at extended hold times as a basis to assess the accuracy of abbreviated equilibration criteria. However, the mass measurement accuracy at extended times depends on the operational stability of the instrument. Published data on the stability of automated sorption balances are rare. An interlaboratory study was undertaken to investigate equilibration criteria for automated sorption balances. This paper focuses on the mass, temperature, and RH stability and includes data from 25 laboratories throughout the world. An initial target for instrument mass stability was met on the first attempt in many cases, but several instruments were found to have unexpectedly large instabilities. The sources of these instabilities were investigated and greatly reduced. This paper highlights the importance of verifying operational mass stability of automated sorption balances, gives a method to perform stability checks, and provides guidance on identifying and correcting common sources of mass instability.

AB - Automated sorption balances are widely used for characterizing the interaction of water vapor with hygroscopic materials. These instruments provide an efficient way to collect sorption isotherm data and kinetic data. A typical method for defining equilibrium after a step change in relative humidity (RH) is using a particular threshold value for the rate of change in mass with time. Recent studies indicate that commonly used threshold values yield substantial errors and that further measurements are needed at extended hold times as a basis to assess the accuracy of abbreviated equilibration criteria. However, the mass measurement accuracy at extended times depends on the operational stability of the instrument. Published data on the stability of automated sorption balances are rare. An interlaboratory study was undertaken to investigate equilibration criteria for automated sorption balances. This paper focuses on the mass, temperature, and RH stability and includes data from 25 laboratories throughout the world. An initial target for instrument mass stability was met on the first attempt in many cases, but several instruments were found to have unexpectedly large instabilities. The sources of these instabilities were investigated and greatly reduced. This paper highlights the importance of verifying operational mass stability of automated sorption balances, gives a method to perform stability checks, and provides guidance on identifying and correcting common sources of mass instability.

KW - Interlaboratory investigation

KW - Measurement uncertainty

KW - Water vapor sorption

U2 - 10.1007/s10450-024-00472-9

DO - 10.1007/s10450-024-00472-9

M3 - Journal article

AN - SCOPUS:85190371215

JO - Adsorption

JF - Adsorption

SN - 0929-5607

ER -

ID: 390180010