Microplastic analysis requires effective separation and purification methods, which greatly depend on the matrix and target particle size. Microplastics-sediment extraction usually involves intermediate steps, increasing processing time and particle loss, particularly for particles <100 μm. Here, we propose an improved separation and quantification method for fine-grained sediment that minimizes microplastic loss by reducing intermediate steps. First, the sample is treated with CH₃COOH, KOH and NaClO, and only transferred for the density separation (ZnCl₂). The extraction efficiency, visually evaluated on spiked samples, was higher than 90% for particles >100 μm and 83% for 63-75 μm particles. This indicates that a sequential extraction method reduces the risk of particle loss, particularly of the small size fraction. Comparatively, the extraction of ABS particles (20-100 μm) was low (30%) but the recovery, assessed via μFTIR, was higher (55%). Additionally, the proposed method can be adapted to other sediment types and environmental matrices.